HRID719353

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID518622

4,5-Dichlorothiophene-2-sulfonyl chloride

C4HCl3O2S2

HCID2807473

7-Methoxy-4,5-dihydronaphtho[1,2-d][1,3]thiazol-2-amine--hydrogen bromide (1/1)

C12H13BrN2OS

PRODUCTS

生成物

结构：COc1ccc2c(c1)CCc1sc(NS(=O)(=O)c3cc(Cl)c(Cl)s3)nc1-2

HCID10114591

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 7-methoxy-4,5-dihydronaphtho(1,2-D)(1,3)thiazol-2-amine hydrobromide (85 mg) and 2,3-dichlorothiophene-5-sulfonyl chloride (68 mg) as described in the synthetic METHOD B to give a white solid (16.4 mg) with purity >90%: MS (pos) m/z 447.3, 449.3.