HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Chloro-2-thienyl)-1,3-thiazol-2-amine → HCID 10299227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Chloro-2-thienyl)-1,3-thiazol-2-amine | HCID 1488441 | — |
| Reactant | 4-Bromo-5-chlorothiophene-2-sulfonyl chloride | HCID 2797220 | — |
| Product | HCID 10299227 | HCID 10299227 | — |
Reaction Steps
The title compound was prepared from 4-(3-chloro-2-thienyl)-1,3-thiazol-2-amine (59 mg) and 4-bromo-5-chlorothiophene-2-sulfonyl chloride (80 mg) as described in the synthetic METHOD B to give a white solid (34.2 mg) with purity >90%: MS (pos) m/z 457.1, 477.1, 479.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-a3acaac8b8f14541a41016c2e96e7d76 |
| Source note | uspto-grants-2006_11 |