HRID719358

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2737400

3-bromo-5-chlorothiophene-2-sulfonyl chloride

C4HBrCl2O2S2

HCID2807473

7-Methoxy-4,5-dihydronaphtho[1,2-d][1,3]thiazol-2-amine--hydrogen bromide (1/1)

C12H13BrN2OS

PRODUCTS

生成物

结构：COc1ccc2c(c1)CCc1sc(NS(=O)(=O)c3sc(Cl)cc3Br)nc1-2

HCID10163539

未命名化合物

PROCEDURE

实验过程

The title compound was prepared 7-methoxy-4,5-dihydronaphtho(1,2-D)(1,3)thiazol-2-amine hydrobromide (85 mg) and 3-bromo-5-chlorothiophene-2-sulfonyl chloride (80 mg) as described in the synthetic METHOD B to give a white solid (17.8 mg) with purity >80%: MS (pos) m/z 491.3, 493.3.