HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,5-difluorobenzenesulfonyl Chloride → HCID 10209980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,5-difluorobenzenesulfonyl Chloride | HCID 574590 | — |
| Reactant | HCID 628563 | HCID 628563 | — |
| Product | HCID 10209980 | HCID 10209980 | — |
Reaction Steps
The title compound was prepared 4-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1,3-thiazol-2-amine (85 mg) and 4-bromo-2,5-difluorobenzenesulfonyl chloride (79 mg) as described in the synthetic METHOD B to give a white solid (38.2 mg) with purity >90%: MS (pos) m/z 567.2, 569.2, 571.2; MS (neg) m/z 565.5, 567.5, 569.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-ceedfb2b9789401c964732e6ea4260a2 |
| Source note | uspto-grants-2006_11 |