HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-N-Propylbenzenesulphonyl chloride → N-(4,5-dihydrothieno[3,2-e][1,3]benzothiazol-2-yl)-4-propylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-N-Propylbenzenesulphonyl chloride | HCID 2737222 | — |
| Reactant | 5,10-Dithia-3-azatricyclo[7.3.0.0,2,6]dodeca-1(9),2(6),3,11-tetraen-4-amine | HCID 21898195 | — |
| Product | N-(4,5-dihydrothieno[3,2-e][1,3]benzothiazol-2-yl)-4-propylbenzenesulfonamide | HCID 10135012 | — |
Reaction Steps
The title compound was prepared from 4,5-dihydrothieno[3,2-e][1,3]benzothiazol-2-amine (105 mg, synthesized according to METHOD I from 4-keto-4,5,6,7-tetrahydrothianaphthene) and 4-n-propylbenzenesulfonyl chloride (111 mg) as described in the synthetic METHOD A to give a white powder (18 mg) with a purity >90%: MS-ES (neg) m/z 389.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-9ace31efa6e34e51bd0989f6522abf32 |
| Source note | uspto-grants-2006_11 |