HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-N-Propylbenzenesulphonyl chloride → HCID 10274239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-N-Propylbenzenesulphonyl chloride | HCID 2737222 | — |
| Reactant | HCID 9992165 | HCID 9992165 | — |
| Product | HCID 10274239 | HCID 10274239 | — |
Reaction Steps
The title compound was prepared from 8-nitro-4,5-dihydronaphtho[1,2-d][1,3]thiazol-2-amine (100 mg, synthesized according to METHOD I from 7-nitrotetralone) and 4-n-propylbenzenesulfonyl chloride (106 mg) as described in the synthetic METHOD A to give a yellow powder (3.5 mg) with a purity of 87%: MS-ES (neg) m/z 428.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-b7abef8e53e3452ba49924e6e542c658 |
| Source note | uspto-grants-2006_11 |