HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 11429136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | HCID 9992165 | HCID 9992165 | — |
| Product | HCID 11429136 | HCID 11429136 | — |
Reaction Steps
The title compound was prepared from 8-nitro-4,5-dihydronaphtho[1,2-d][1,3]thiazol-2-amine (100 mg, synthesized according to METHOD I from 7-nitrotetralone) and benzenesulfonyl chloride (85 mg) as described in the synthetic METHOD A to give a yellow powder (12 mg) with a purity of >90%: MS-ES (neg) m/z 386.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-97e59e794b3e402c9429913e4af03c55 |
| Source note | uspto-grants-2006_11 |