HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86595355, compound → HCID 86595356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86595355 | HCID 86595355 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86595356 | HCID 86595356 | — |
Reaction Steps
3 g (0.093 mol) of 1-methyl-3-[1-(4-nitrophenyl)pyrrolidin-2-ylmethyl]-3H-imidazol-1-ium (2) dissolved in 350 ml of ethanol were hydrogenated in the presence of palladium-on-charcoal under a hydrogen pressure of 10 bar at a temperature of 30° C.; after filtering off the catalyst, the expected derivative (3) was isolated in the form of the hydrochloride. 2.6 g of a white powder were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132543B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-002f2343ffa64d27b57423481489db5b |
| Source note | uspto-grants-2006_11 |