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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 719834Generated: October 31, 2026

Citric Acid → HCID 21887943, compound

https://huagongshe.com/reaction/719834

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCitric AcidHCID 311—
ReactantHCID 21887313HCID 21887313—
ProductHCID 21887943HCID 21887943—

Reaction Steps

Using 8-(5-{[2-(2-chlorophenyl)ethyl]amino}pentanoyl)-5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-2 (1H)-one hydrochloride (205 mg, 0.5 mmol) obtained in Example 39 and citric acid (96 mg, 0.5 mmol) according to the same method as that of Example 360, the title compound was obtained as colorless crystals (278 mg) having a melting point of 100 to 102° C. (dec).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07132547B2
Source datasetuspto-grants-2006_11
ORD IDord-bbd3419cf185448a8aeb9a898e59fa20
Source noteuspto-grants-2006_11