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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 720091Generated: October 30, 2026

Trifluoroacetic acid → HCID 137241990, compound

https://huagongshe.com/reaction/720091

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 136181670HCID 136181670—
SolventDichloromethaneHCID 6344—
ProductHCID 137241990HCID 13724199091%

Reaction Steps

Preparation of example 32 from the title compound of Example 30 (31 mg, 0.062 mmol) and 45% TFA in CH2Cl2 (1 mL) was carried out analogously to Example 20. Isolation, also in an analogous manner, afforded the title compound (29 mg, 0.056 mmol) as a yellow powder in 91% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07132533B2
Source datasetuspto-grants-2006_11
ORD IDord-94c7965f14df44e8acc39631ee83359a
Source noteuspto-grants-2006_11