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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 720143Generated: October 30, 2026

Hydrochloric Acid → HCID 136401843, compound

https://huagongshe.com/reaction/720143

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 136181624HCID 136181624—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 136401843HCID 13640184397%

Reaction Steps

Preparation of example 179 from the title compound of Example 158 (57 mg, 0.115 mmol) and 4M HCl in dioxane (10 mL) was carried out analogously to Example 91. Isolation, also in an analogous manner afforded the title compound (48 mg, 0.111 mmol) as an orange/yellow powder in 97% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07132533B2
Source datasetuspto-grants-2006_11
ORD IDord-440146f661244fe281defdd7834d1516
Source noteuspto-grants-2006_11