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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 720146Generated: October 29, 2026

Hydrochloric Acid → HCID 136341287, compound

https://huagongshe.com/reaction/720146

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 136181672HCID 136181672—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 136341287HCID 13634128780%

Reaction Steps

Preparation of example 194 from the title compound of Example 157 (48 mg, 0.10 mmol) and 4M HCl in dioxane (10 mL) was carried out analogously to Example 91. Isolation, also in an analogous manner afforded the title compound (34 mg, 0.08 mmol) as an orange/yellow powder in 80% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07132533B2
Source datasetuspto-grants-2006_11
ORD IDord-3a5e515989c84c02baf01cce91f20916
Source noteuspto-grants-2006_11