Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Fluoro-3-nitrobenzene | HCID 9823 | — |
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 21889076 | HCID 21889076 | — |
Reaction Steps
28.2 g 3-fluoronitrobenzene and 137.5 g 1-(3-aminopropyl)imidazole were dissolved in 300 ml dimethyl sulfoxide, and the batch was stirred for 60 h at 100° C. After cooling, the batch was poured into 1 l water. The precipitated product was suction-filtered and dried overnight under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07135047B2 |
|---|
| Source dataset | uspto-grants-2006_11 |
|---|
| ORD ID | ord-61b9d81092d04804a2c2bcf8b1c8c151 |
|---|
| Source note | uspto-grants-2006_11 |
|---|
