HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 21891665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 21891668 | HCID 21891668 | — |
| Reactant | HCID 60090632 | HCID 60090632 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 21891665 | HCID 21891665 | — |
Reaction Steps
Preparation takes place in analogy to that described in Example 7 A from 1.50 g (9.48 mmol) of 1-(2,3-difluorobenzyl)hydrazine from Example 2 A, 1.55 g (9.48 mmol) of sodium (1E)-1-cyano-3-ethoxy-3-oxo-1-propen-2-olate from Example 6 A, 1.73 g (1.17 ml; 15.18 mmol) of trifluoroacetic acid and 40 ml of dioxane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135474B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-fb62cbaf424148c5ab56a80c0d80e285 |
| Source note | uspto-grants-2006_11 |