Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 720253Generated: October 28, 2026

Trifluoroacetic acid → HCID 21891665, compound

https://huagongshe.com/reaction/720253

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 21891668HCID 21891668—
ReactantHCID 60090632HCID 60090632—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 21891665HCID 21891665—

Reaction Steps

Preparation takes place in analogy to that described in Example 7 A from 1.50 g (9.48 mmol) of 1-(2,3-difluorobenzyl)hydrazine from Example 2 A, 1.55 g (9.48 mmol) of sodium (1E)-1-cyano-3-ethoxy-3-oxo-1-propen-2-olate from Example 6 A, 1.73 g (1.17 ml; 15.18 mmol) of trifluoroacetic acid and 40 ml of dioxane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07135474B2
Source datasetuspto-grants-2006_11
ORD IDord-fb62cbaf424148c5ab56a80c0d80e285
Source noteuspto-grants-2006_11