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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 720454Generated: October 30, 2026

Potassium cyanate → HCID 135828228, compound

https://huagongshe.com/reaction/720454

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium cyanateHCID 11378442—
ReactantHCID 135828224HCID 135828224—
CatalystMethanolHCID 887—
SolventHydrochloric AcidHCID 313—
ProductHCID 135828228HCID 135828228—

Reaction Conditions

Temperature50 °C

Reaction Steps

31.1 mg (0.1 mmol) of 2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile are suspended in 0.91 ml of 1N HCl, and 8.1 mg (0.1 mmol) of potassium cyanate are added. After the addition of a few drops of methanol, the mixture is stirred at 50° C. for a total of 10 hours. The crystals are filtered off with suction and washed with water and ether.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07135486B1
Source datasetuspto-grants-2006_11
ORD IDord-3da9867df2ef47d6ba0c6f4eaec10340
Source noteuspto-grants-2006_11