HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 720464Generated: October 25, 2026
Hydrochloric Acid → HCID 178474088, compound
https://huagongshe.com/reaction/720464
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Sulfide | HCID 14804 | — |
| Reactant | N-{4-[2-Amino-3,5-dicyano-6-(phenylsulphanyl)-4-pyridinyl]phenyl}acetamide | HCID 12016387 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178474088 | HCID 178474088 | — |
Reaction Steps
Under argon, 1.16 g (3 mmol) of N-{4-[2-amino-3,5-dicyano-6-(phenylsulfanyl)-4-pyridinyl]phenyl}-acetamide are dissolved in 10 ml of DMF, 0.78 g (10 mmol) of sodium sulfide are added and the mixture is stirred at 80° C. for 2 h. 20 ml of 1N HCl are then added and the resulting crystals are filtered off with suction and dried under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07135486B1 |
|---|
| Source dataset | uspto-grants-2006_11 |
|---|
| ORD ID | ord-2398b58de3f04f3cb6df7b032dad8cda |
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| Source note | uspto-grants-2006_11 |
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