HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 69613552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Reactant | HCID 21892828 | HCID 21892828 | — |
| Product | HCID 69613552 | HCID 69613552 | — |
Reaction Steps
The mixture of Example 38C (140 mg, 0.332 mmol) and 3-bromopyridine (0.042 mL, 0.43 mmol) were processed as described in Example 4C. Purification by chromatography (SiO2, 30% EtOAc/hexane) provided 90 mg (85%) of a 4:1 mixture of the title compounds. MS (DCI/NH3) m/z 321 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135484B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-075fa74c95874ad0b2628662f0d77499 |
| Source note | uspto-grants-2006_11 |