HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromopyridine → HCID 21892701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Reactant | rel-1,1-Dimethylethyl (3aR,6aS)-hexahydro-4-oxocyclopenta[c]pyrrole-2(1H)-carboxylate | HCID 29948688 | — |
| Product | HCID 21892701 | HCID 21892701 | 27% |
Reaction Steps
3-Bromopyridine (4.36 g, 27.6 mmol) and the product from Example 44A (2.07 g, 9.19 mmol) were processed as described in Example 1E to afford the title compound (0.743 g, 27%). MS (DCI/NH3) m/z 305 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135484B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-6caac7f76e4848cc80d8020d32b82c90 |
| Source note | uspto-grants-2006_11 |