HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 10457781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | N,N′-[4-[[3-Butyl-1-[(2-fluorophenyl)methyl]-2,3,6,9-tetrahydro-2,6-dioxo-1H-purin-8-yl]methyl]-1,3-phenylene]bis[acetamide] | HCID 44427026 | — |
| Product | HCID 10457781 | HCID 10457781 | — |
Reaction Steps
Prepared from N-{3-acetylamino-4-[3-butyl-1-(2-fluorobenzyl)-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-ylmethyl]-phenyl}-acetamide by refluxing with 20% aqueous potassium hydroxide. The product was purified by chromatography using silica eluted with 92:8 chloroform/methanol. MS, m/z(M+)=478.2132.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135475B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-24fbe581c818492bb944dcad393ae7f6 |
| Source note | uspto-grants-2006_11 |