HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octene → HCID 21895230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octene | HCID 8125 | — |
| Reactant | HCID 178527039 | HCID 178527039 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21895230 | HCID 21895230 | 98% |
Reaction Steps
In toluene (2 ml)under a nitrogen atmosphere at 100° C. for 20 hours, 1 mmol of cyclohexyl phenylphosphinate and 1 mmol of 1-octene were allowed to react using 3 molar % of Rh(PPh3)3Br as a catalyst to give cyclohexyl phenyl[(E)-1-octen-1-yl]phosphinate in a yield of 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135583B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-51fb554d2f124358bf4afe1bbb6a8f91 |
| Source note | uspto-grants-2006_11 |