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HRID722016

反应详情

EQUATION

反应方程式

HRID 722016 的结构方程式

REACTANTS

反应物

3
结构：CI
HCID6328

Methyl iodide

CH3I

结构：CC(C)[N-]C(C)C.[Li+]
HCID2724682

2-Propanamine, N-(1-methylethyl)-, lithium salt

C6H14LiN

结构：COC(=O)C1CCC2(CC1)OCCO2
HCID10845708

Methyl 1,4-dioxaspiro[4.5]decane-8-carboxylate

C10H16O4

PRODUCTS

生成物

1
结构：COC(=O)C1(C)CCC2(CC1)OCCO2
HCID22591390

Methyl 8-methyl-1,4-dioxaspiro[4.5]decane-8-carboxylate

C11H18O4

PROCEDURE

实验过程

According to the process described in the literature (JP83-118577), methyl 1,4-dioxaspiro [4.5]decan-8-carboxylate was reacted with methyl iodide in the presence of LDA (lithium diisopropylamide) to obtain methyl 8-methyl-1,4-dioxaspiro [4.5]decan-8-carboxylate (the compound (1) of the above figure).