HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-3-nitro-5-cyclohexylmethyl-pyridine → 2-Amino-3-nitro-5-cyclohexylmethyl-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-3-nitro-5-cyclohexylmethyl-pyridine | HCID 21882723 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | 2-Amino-3-nitro-5-cyclohexylmethyl-pyridine | HCID 21882723 | — |
| Product | HCID 21882760 | HCID 21882760 | — |
Reaction Steps
Similiarly to Example C1, the hydrogenation of 0.365 g of 2-amino-3-nitro-5-cyclohexylmethyl-pyridine (starting material E2) gives 0.29 g of the title compound as a dark powder (after chromatography with dichloromethane/methanol 99:1). The mass spectrum shows the molecular peak MH+ at 205 Da.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138399B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-f82e2bbfa90046c5b5d2ce8b79de1e5f |
| Source note | uspto-grants-2006_11 |