HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 722089Generated: October 29, 2026
Potassium Carbonate → HCID 21882971, compound
https://huagongshe.com/reaction/722089
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 21882859 | HCID 21882859 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21882971 | HCID 21882971 | — |
Reaction Steps
A suspension of 6-chloro-9-(5-acetoxy-4-acetoxymethyl-6-methyl-pyridin-3-ylmethyl)-9H-purin-2-ylamine and K2CO3 (excess) in MeOH was heated to 50° C. for 15 min. Filtration, work-up (EtOAc) and purification by preparative TLC gave the title compound. HPLC Rt: 4.498 min. 1H-NMR (d6-DMSO) δ 8.08 (s, 1H), 7.74 (s, 1H), 6.95 (s, 1H), 5.31 (s, 2H), 4.74 (s, 2H), 2.31 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07138401B2 |
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| Source dataset | uspto-grants-2006_11 |
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| ORD ID | ord-1849f39cab224590af86f699f10258f9 |
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| Source note | uspto-grants-2006_11 |
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