HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → tert-Butyl 4-(4-nitrophenyl)-1,4-diazepane-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | Tert-butyl 1,4-diazepane-1-carboxylate | HCID 2756058 | — |
| Product | tert-Butyl 4-(4-nitrophenyl)-1,4-diazepane-1-carboxylate | HCID 18008978 | — |
Reaction Steps
[1,4]Diazepane-1-carboxylic acid tert-butyl ester was reacted with 1-Fluoro-4-nitro-benzene at 60° C. by method D. The product with the molecular weight of 321.38 (C16H23N3O4) was obtained in this way; MS (ESI): 322 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08828991B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-852f1a1370e14c52b49b720a861f560f |
| Source note | uspto-grants-2014_09 |