HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride, 3,4,5-trimethoxy- → HCID 21883046, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride, 3,4,5-trimethoxy- | HCID 78282 | — |
| Reactant | 6-chloro-1H-purin-2-amine | HCID 178508435 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21883046 | HCID 21883046 | — |
Reaction Steps
A solution of 6-chloro-9H-purin-2-ylamine in pyridine was treated with 3,4,5-trimethoxybenzoyl chloride at r.t. for 2 h. Work-up and purification by preparative TLC (EtOAc:hexane 1:1) gave the title compound. HPLC Rt: 5.305 min. 1H-NMR (CDCl3): δ 8.24 (s, 1H), 7.13 (s, 2H), 5.36 (s, 2H), 3.99 (s, 3H), 3.88 (s, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138401B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-05786054ba9b4f23889aae1fe9db821f |
| Source note | uspto-grants-2006_11 |