HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Methylhydroxylamine hydrochloride → 9-(3-Chloro-2,6-difluorobenzyl)-N-methoxy-9H-beta-carboline-3-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Reactant | 9-(3-chloro-2,6-difluorobenzyl)-9H-beta-carboline-3-carboxylic acid | HCID 21883394 | — |
| Product | 9-(3-Chloro-2,6-difluorobenzyl)-N-methoxy-9H-beta-carboline-3-carboxamide | HCID 10046640 | — |
Reaction Steps
The title compound is prepared by coupling of 9-(3-chloro-2,6-difluorobenzyl)-9H-β-carboline-3-carboxylic acid and O-methyl hydroxylamine hydrochloride under conditions similar to those provided in step (b) of example 7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138408B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-a04da0cf29f6400cad1addd382fcd340 |
| Source note | uspto-grants-2006_11 |