Dimethylformamide dimethyl acetal → HCID 68978518, compound

HRID 72219Notes

Reaction equation

HRID 72219 reaction equation
[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([C:11]([CH:13]2[CH2:18][CH2:17][O:16][CH2:15][CH2:14]2)=[O:12])=[CH:8][C:9]=1[NH2:10])=[O:4].CO[CH:21]([N:24]([CH3:26])[CH3:25])OC>>[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([C:11]([CH:13]2[CH2:18][CH2:17][O:16][CH2:15][CH2:14]2)=[O:12])=[CH:8][C:9]=1[N:10]=[CH:21][N:24]([CH3:26])[CH3:25])=[O:4]

Participants

3

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 68976824HCID 68976824, compound

Product 1

HCID 68978518HCID 68978518, compound

Procedure

3-Amino-5-(tetrahydropyran-4-carbonyl)thiophene-2-carboxylic acid methyl ester and dimethoxymethyldimethylamine were reacted by method B. The product with the molecular weight of 324.40 (C15H20N2O4S) was obtained in this way; MS (ESI): 325 (M+H+).

Workup

  1. customThe product with the molecular weight of 324.40 (C15H20N2O4S) was obtained in this way

Sources & evidence

ORD record
ord-c377a92b5c1e4620a14f2f9e16c00e01
Source dataset
uspto-grants-2014_09
Patent number
US08828991B2

Reaction notes

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