HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178488183, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178470789 | HCID 178470789 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178488183 | HCID 178488183 | — |
Reaction Steps
The mixture of 140 mg of ethyl [5-(3-methoxy-4-nitrophenyl)-4H-[1,2,4]triazol-3-yl]acetate, 5 ml of methanol and 1 ml of 1N sodium hydroxide was stirred at room temperature for 2 hours. Afterwards, the volatile fractions are removed on a rotary evaporator, the residue is diluted with 10 ml of water and adjusted to pH 5 using 1N hydrochloric acid. The solid was filtered off with suction after the stirring.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138414B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-b3f705ec3fb846679e7edcc61372e661 |
| Source note | uspto-grants-2006_11 |