HRID722205

反应详情

EQUATION

反应方程式

HRID 722205 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The solution of equivalent amounts of 2-chloro-4-fluorobenzoyl isocyanate in acetonitrile was added dropwise to the solution of 89 mg of [5-(3-methoxy-4-nitrophenyl)-4H-[1,2,4]triazol-3-yl]acetate in 5 ml of acetonitrile and the mixture was stirred at room temperature overnight. The solid formed was then filtered off with suction and dried under reduced pressure.

WORKUP

后处理

  1. customThe solid formed
  2. filtrationwas then filtered off with suction
  3. customdried under reduced pressure