HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isocyanate, 2-chloro-4-fluoro- → HCID 178488181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isocyanate, 2-chloro-4-fluoro- | HCID 11521269 | — |
| Reactant | HCID 178488182 | HCID 178488182 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178488181 | HCID 178488181 | — |
Reaction Steps
The solution of equivalent amounts of 2-chloro-4-fluorobenzoyl isocyanate in acetonitrile was added dropwise to the solution of 89 mg of [5-(3-methoxy-4-nitrophenyl)-4H-[1,2,4]triazol-3-yl]acetate in 5 ml of acetonitrile and the mixture was stirred at room temperature overnight. The solid formed was then filtered off with suction and dried under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138414B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-dae1b33701a9447e952ac0bccac2edd9 |
| Source note | uspto-grants-2006_11 |