Tin tetrachloride → HCID 178433948, compound

Participants

Reaction Steps

The mixture consisting of 120 mg of 3-(4-chloro-3-nitrophenyl)-5-methyl-4H-[1,2,4]triazole, 30 ml of ethyl acetate and 644 mg of tin chloride was heated to reflux for 6 hours. After cooling, the mixture was washed with water, and the organic phase was dried over sodium sulfate and concentrated at 40° C. under reduced pressure.

Provenance & Evidence