HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4,5-difluorobenzoyl Isocyanate → HCID 178433949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4,5-difluorobenzoyl Isocyanate | HCID 11557583 | — |
| Reactant | HCID 178433948 | HCID 178433948 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178433949 | HCID 178433949 | — |
Reaction Steps
The solution of equivalent amounts of 2-chloro-4,5-difluorobenzoyl isocyanate was added dropwise to the solution of 85 mg of 3-(3-amino-4-chlorophenyl)-5-methyl-4H-1,2,4-triazole in 8 ml of acetonitrile and the mixture was stirred at room temperature for 2 hours. The solid formed is then filtered off with suction and dried under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138414B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-5d1a2a01d5114bea9f91e89a8ae4a86c |
| Source note | uspto-grants-2006_11 |