HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(1H-benzimidazol-2-yl)aniline → HCID 21883861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(1H-benzimidazol-2-yl)aniline | HCID 79869 | — |
| Reactant | 2-Chloro-4,5-difluorobenzoyl Isocyanate | HCID 11557583 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 21883861 | HCID 21883861 | — |
Reaction Steps
The solution of equivalent amounts of 2-chloro-4,5-difluorobenzoyl isocyanate was added dropwise to the solution of 142 mg of 2-(1H-benzimidazol-2-yl)phenylamine in 8 ml of acetonitrile and the mixture was stirred at room temperature for 30 minutes. The solid was then filtered off with suction and dried under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138414B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-e08d567c9c1549fa86ac375ec65cca48 |
| Source note | uspto-grants-2006_11 |