Tin tetrachloride → 3-(3-Amino-4-chlorophenyl)-6-methyl-1,2,4-triazin-5(2H)-one

HRID 722228Notes

Reaction equation

HRID 722228 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[NH:13][C:12](=[O:14])[C:11]([CH3:15])=[N:10][N:9]=2)=[CH:4][C:3]=1[N+:16]([O-])=O.[Sn](Cl)(Cl)(Cl)Cl>>[NH2:16][C:3]1[CH:4]=[C:5]([C:8]2[NH:13][C:12](=[O:14])[C:11]([CH3:15])=[N:10][N:9]=2)[CH:6]=[CH:7][C:2]=1[Cl:1]

Participants

3

Reactant 2

HCID 24287Tin tetrachlorideHCID 1358393733-(4-Chloro-3-nitrophenyl)-6-methyl-1,2,4-triazin-5(2H)-one

Product 1

HCID 1358393793-(3-Amino-4-chlorophenyl)-6-methyl-1,2,4-triazin-5(2H)-one

Procedure

This compound was obtained by reducing 3-(4-chloro-3-nitrophenyl)-6-methyl-4H-[1,2,4]triazin-5-one with tin chloride.

Workup

  1. customThis compound was obtained

Sources & evidence

ORD record
ord-5198333efc2f47ce8106b680bf2401dc
Source dataset
uspto-grants-2006_11
Patent number
US07138414B2

Reaction notes

Loading…