Tin tetrachloride → 2-Chloro-5-(5,6-dimethyl-1,2,4-triazin-3-yl)aniline

HRID 722229Notes

Reaction equation

HRID 722229 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[N:10][C:11]([CH3:15])=[C:12]([CH3:14])[N:13]=2)=[CH:4][C:3]=1[N+:16]([O-])=O.[Sn](Cl)(Cl)(Cl)Cl>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[N:10][C:11]([CH3:15])=[C:12]([CH3:14])[N:13]=2)=[CH:4][C:3]=1[NH2:16]

Participants

3

Reactant 2

HCID 24287Tin tetrachlorideHCID 218838733-(4-Chloro-3-nitrophenyl)-5,6-dimethyl-1,2,4-triazine

Product 1

HCID 218838862-Chloro-5-(5,6-dimethyl-1,2,4-triazin-3-yl)aniline

Procedure

This compound was obtained by reducing 3-(4-chloro-3-nitrophenyl)-5,6-dimethyl-[1,2,4]triazine with tin chloride.

Workup

  1. customThis compound was obtained

Sources & evidence

ORD record
ord-da04303dbc134e87abd503c3ee8f8279
Source dataset
uspto-grants-2006_11
Patent number
US07138414B2

Reaction notes

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