HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4,5-difluorobenzoyl Isocyanate → HCID 135839375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4,5-difluorobenzoyl Isocyanate | HCID 11557583 | — |
| Reactant | 3-(3-Amino-4-chlorophenyl)-6-methyl-1,2,4-triazin-5(2H)-one | HCID 135839379 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 135839375 | HCID 135839375 | — |
Reaction Steps
The solution of equivalent amounts of 2-chloro-4,5-difluorobenzoyl isocyanate was added dropwise to the solution of 60 mg of 3-(3-amino-4-chlorophenyl)-6-methyl-4H-[1,2,4]triazin-5-one in 8 ml of acetonitrile and the mixture was stirred at room temperature for 30 minutes. The solid was filtered off with suction and dried under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138414B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-c2e24785cb60435685d75a79acee1987 |
| Source note | uspto-grants-2006_11 |