HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → 2-Hydroxy-4-(2-hydroxy-1,1-dimethylethyl)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | HCID 21883735 | HCID 21883735 | — |
| Product | 2-Hydroxy-4-(2-hydroxy-1,1-dimethylethyl)benzaldehyde | HCID 21883724 | — |
Reaction Steps
The phenol (Step 5) was converted to the salicylaldehyde via a method similar to that described in Example 2, Step 1: mp 80.4–81.9° C. 1H NMR (CDCl3/300 MHz) 11.00 (s, 1H), 9.87 (s, 1H), 7.51 (d, 1H, J=8.3 Hz), 7.08 (dd, 1H, J=8.3 Hz, 1.4 Hz), 7.02 (d, 1H, J=1.4 Hz), 3.66 (s, 2H), 1.34 (s, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138411B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-0b89d4aeaa2f4dd190a8241edc60d842 |
| Source note | uspto-grants-2006_11 |