Dimethylformamide dimethyl acetal → HCID 57618749, compound

HRID 72237Notes

Reaction equation

HRID 72237 reaction equation
[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([CH:11]=[O:12])=[CH:8][C:9]=1[NH2:10])=[O:4].CO[CH:15]([N:18]([CH3:20])[CH3:19])OC>>[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([CH:11]=[O:12])=[CH:8][C:9]=1[N:10]=[CH:15][N:18]([CH3:20])[CH3:19])=[O:4]

Participants

3

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 86628786HCID 86628786, compound

Product 1

HCID 57618749HCID 57618749, compound

Procedure

3-Amino-5-formylthiophene-2-carboxylic acid methyl ester and dimethoxymethyldimethylamine were reacted by method B. The product with the molecular weight of 308.40 (C15H20N2O3S) was obtained in this way; MS (ESI): 309 (M+H+).

Workup

  1. customThe product with the molecular weight of 308.40 (C15H20N2O3S) was obtained in this way

Sources & evidence

ORD record
ord-a1d36b149f4a4406b5248e3fb0a1acde
Source dataset
uspto-grants-2014_09
Patent number
US08828991B2

Reaction notes

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