Pyrrolidine → HCID 57625325, compound

HRID 72239Notes

Reaction equation

HRID 72239 reaction equation
[CH3:1][N:2]1[CH2:8][CH2:7][CH2:6][N:5]([C:9]2[CH:14]=[CH:13][C:12]([N:15]3[C:20](=[O:21])[C:19]4[S:22][C:23]([CH:25]=O)=[CH:24][C:18]=4[N:17]=[CH:16]3)=[CH:11][CH:10]=2)[CH2:4][CH2:3]1.[NH:27]1[CH2:31][CH2:30][CH2:29][CH2:28]1>>[CH3:1][N:2]1[CH2:8][CH2:7][CH2:6][N:5]([C:9]2[CH:14]=[CH:13][C:12]([N:15]3[C:20](=[O:21])[C:19]4[S:22][C:23]([CH2:25][N:27]5[CH2:31][CH2:30][CH2:29][CH2:28]5)=[CH:24][C:18]=4[N:17]=[CH:16]3)=[CH:11][CH:10]=2)[CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 31268PyrrolidineHCID 86628970HCID 86628970, compound

Product 1

HCID 57625325HCID 57625325, compound

Procedure

3-[4-(4-Methylperhydro-1,4-diazepin-1-yl)phenyl]-4-oxo-3,4-dihydrothieno[3,2-d]pyrimidine-6-carbaldehyde was reacted with pyrrolidine by method BA. The product with the molecular weight of 423.58 (C23H29N5OS) was obtained in this way; MS (ESI): 424 (M+H+).

Workup

  1. customThe product with the molecular weight of 423.58 (C23H29N5OS) was obtained in this way

Sources & evidence

ORD record
ord-2947f2103c804261bb424534ab8b60ef
Source dataset
uspto-grants-2014_09
Patent number
US08828991B2

Reaction notes

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