HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylphenylboronic acid → HCID 21884534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylphenylboronic acid | HCID 2734310 | — |
| Reactant | 2-(3-Nitro-4-methoxyphenyl)-5-bromobenzoxazole | HCID 21884342 | — |
| Product | HCID 21884534 | HCID 21884534 | — |
Reaction Steps
Prepared by the method of Example 15d), from 2-(3-nitro-4-methoxyphenyl)-5-bromobenzoxazole (200 mg, 0.57 mmol) and 3-acetylphenylboronic acid (139 mg, 0.85 mmol) the subtitle compound was obtained (89 mg, 26%). 1H NMR (DMSO) δ 8.75(d, 1H), 8.46(dd, 1H), 8.23(t, 1H), 7.98–7.96(m, 2H), 7.69–7.56(m, 3H), 7.27(d, 1H), 4.08(s, 3H), 2.68(s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-f92c68b4abfd44f093514d5461e0f31d |
| Source note | uspto-grants-2006_11 |