Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 722495Generated: October 31, 2026

3-Acetylphenylboronic acid → HCID 21884534, compound

https://huagongshe.com/reaction/722495

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Acetylphenylboronic acidHCID 2734310—
Reactant2-(3-Nitro-4-methoxyphenyl)-5-bromobenzoxazoleHCID 21884342—
ProductHCID 21884534HCID 21884534—

Reaction Steps

Prepared by the method of Example 15d), from 2-(3-nitro-4-methoxyphenyl)-5-bromobenzoxazole (200 mg, 0.57 mmol) and 3-acetylphenylboronic acid (139 mg, 0.85 mmol) the subtitle compound was obtained (89 mg, 26%). 1H NMR (DMSO) δ 8.75(d, 1H), 8.46(dd, 1H), 8.23(t, 1H), 7.98–7.96(m, 2H), 7.69–7.56(m, 3H), 7.27(d, 1H), 4.08(s, 3H), 2.68(s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07138425B2
Source datasetuspto-grants-2006_11
ORD IDord-f92c68b4abfd44f093514d5461e0f31d
Source noteuspto-grants-2006_11