HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Nitro-6-methoxyphenyl)-5-phenylbenzoxazole → 2-(3-Amino-6-methoxyphenyl)-5-phenylbenzoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Nitro-6-methoxyphenyl)-5-phenylbenzoxazole | HCID 21884386 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 2-(3-Amino-6-methoxyphenyl)-5-phenylbenzoxazole | HCID 21884457 | — |
Reaction Steps
Prepared by the method of Example 15e), from palladium (10 mol %) on carbon and 2-(3-nitro-6-methoxyphenyl)-5-phenylbenzoxazole (450 mg, 1.3 mmol) the subtitle compound was obtained (420 mg, 99%). The product was used directly in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-f9788927e70c458b94df1968c9ca1976 |
| Source note | uspto-grants-2006_11 |