HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Fluoro-5-nitrophenyl)-5-phenylbenzoxazole → HCID 21884372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Fluoro-5-nitrophenyl)-5-phenylbenzoxazole | HCID 21884334 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 21884372 | HCID 21884372 | — |
Reaction Steps
Prepared by the method of Example 44a), from 2-(2-fluoro-5-nitrophenyl)-5-phenylbenzoxazole (200 mg, 0.6 mmol) in butanol (2 ml) the subtitle compound was obtained (195 mg, 87%). 1H NMR (DMSO) δ 8.87(d, 1H), 8.45(dd, 1H), 8.08(d, 1H), 7.85(d, 1H), 7.70(m, 3H), 7.51(t, 3H), 7.40(t, 1H), 4.35(t, 2H), 1.83(q, 2H), 1.57(m, 2H), 1.01(t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-06ada23d45b041819de4240fda581d1c |
| Source note | uspto-grants-2006_11 |