HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Fluoro-5-nitrophenyl)-5-phenylbenzoxazole → 2-(5-Nitro-2-isopropoxyphenyl)-5-phenylbenzoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Fluoro-5-nitrophenyl)-5-phenylbenzoxazole | HCID 21884334 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 2-(5-Nitro-2-isopropoxyphenyl)-5-phenylbenzoxazole | HCID 21884584 | — |
Reaction Steps
Prepared by the method of Example 44a), from 2-(2-fluoro-5-nitrophenyl)-5-phenylbenzoxazole (200 mg, 0.6 mmol) and isopropanol (2 ml) the subtitle compound was obtained (204 mg, 84%). 1H NMR (DMSO) δ 8.85(d, 1H), 8.44(dd, 1H), 8.12(d, 1H), 7.90(d, 1H), 7.76(m, 3H), 7.54(m, 3H), 7.40(t, 1H), 4.35(m, 1H), 1.45(d, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-bda7f9244f8940bb82f9e4130ea95638 |
| Source note | uspto-grants-2006_11 |