HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 2-Fluoro-5-nitrobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2-Fluoro-5-nitrobenzoic acid | HCID 280997 | — |
| Product | 2-Fluoro-5-nitrobenzoyl chloride | HCID 10976570 | — |
Reaction Steps
Prepared by then method of Example 15a), from 2-fluoro-5-nitrobenzoic acid (2.0 g, 11.0 mmol) and oxalyl chloride (2.89 ml, 33.0 mmol) the subtitle compound was obtained. The product was used directly in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-8fca0ace76a64af6880e1d947ff249e0 |
| Source note | uspto-grants-2006_11 |