Propylamine → HCID 21884615, compound

Participants

Reaction Steps

Prepared by the method of Example 54a), from 2-(3-nitro-6-fluorophenyl)-5-chlorobenzoxazole (263 mg, 0.9 mmol) and propylamine (400 μL, 5.0 mmol) the subtitle compound was obtained (296 mg, 99%). 1H NMR (DMSO) δ 9.33(t, 1H), 9.02(s, 1H), 8.44(dd, 1H), 8.16–8.11(m, 2H), 7.75(dd, 1H), 7.29(d, 1H), 3.67(q, 2H), 1.97(m, 2H), 1.28(t, 3H).

Provenance & Evidence