HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86590808, compound → HCID 69706967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86590808 | HCID 86590808 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69706967 | HCID 69706967 | — |
Reaction Steps
(4S,7S,11aR)-7-benzoylamino-6-oxo-1,3,4,6,7,8,11,11a-octahydro-2H-pyrido[1,2-a]azocine-4-carboxylic acid (2-hydroxy-5-oxo-tetrahydrofuran-3-yl)-amide, 46, is dissolved in EtOAc and treated with a catalytic amount of Pd/C. The resulting suspension is stirred at room temperature under a H2 atmosphere for 2 hours. The solution is filtered to remove the catalyst and concentrated in vacuo to afford the desired product
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138395B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-9997cd836a0a4efaaadfc76b64b7eb3e |
| Source note | uspto-grants-2006_11 |