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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 722735Generated: October 31, 2026

HCID 86590808, compound → HCID 69706967, compound

https://huagongshe.com/reaction/722735

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86590808HCID 86590808—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 69706967HCID 69706967—

Reaction Steps

(4S,7S,11aR)-7-benzoylamino-6-oxo-1,3,4,6,7,8,11,11a-octahydro-2H-pyrido[1,2-a]azocine-4-carboxylic acid (2-hydroxy-5-oxo-tetrahydrofuran-3-yl)-amide, 46, is dissolved in EtOAc and treated with a catalytic amount of Pd/C. The resulting suspension is stirred at room temperature under a H2 atmosphere for 2 hours. The solution is filtered to remove the catalyst and concentrated in vacuo to afford the desired product

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07138395B2
Source datasetuspto-grants-2006_11
ORD IDord-9997cd836a0a4efaaadfc76b64b7eb3e
Source noteuspto-grants-2006_11