Hydroxylamine → HCID 58743260, compound

HRID 722821Notes

Reaction equation

HRID 722821 reaction equation
C([N:8]([C@@H:16]([C@@H:18]([OH:34])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33])[CH3:17])CC1C=CC=CC=1)C1C=CC=CC=1.NO>>[NH2:8][C@@H:16]([C@@H:18]([OH:34])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33])[CH3:17]

Participants

3

Reactant 2

HCID 787HydroxylamineHCID 58743387HCID 58743387, compound

Product 1

HCID 58743260HCID 58743260, compoundYield 111.4%

Procedure

According to the method of Example 27, from N,N-dibenzylamine 80 (256 mg, 0.55 mmol), aminoalcohol 81was obtained as a white solid (175 mg, 92% yield).

Sources & evidence

ORD record
ord-24226a5b495b42b980438ab5422ca30f
Source dataset
uspto-grants-2006_11
Patent number
US07138547B2

Reaction notes

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