Hydrochloric Acid → HCID 86760300, compound

Participants

Reaction Steps

To a solution of N-Boc derivative 96 (22 mg, 0.057 mmol) in dioxane (0.4 mL), anhydrous HCl solution in dioxane (5.3M, 0.43 mL, 2.29 mmol) was added. After stirring at room temperature for 5 h, the solvent was removed in vacuo. The resulting solid was washed with dioxane to obtain dihydrochloride 97 as a white solid (11.5 mg, 56% yield).

Provenance & Evidence