5-Chlorovaleryl chloride → HCID 21887081, compound
Reaction equation
[O:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][CH2:2]1.[Cl:11][CH2:12][CH2:13][CH2:14][CH2:15][C:16](Cl)=[O:17]>>[Cl:11][CH2:12][CH2:13][CH2:14][CH2:15][C:16]([C:7]1[CH:6]=[C:5]2[C:10](=[CH:9][CH:8]=1)[O:1][CH2:2][CH2:3][CH2:4]2)=[O:17]Participants
3
Procedure
Using chroman (5.40 g) and 5-chlorovaleryl chloride (6.82 g) according to the same method as that of Reference Example 1, the title compound was obtained as a fine yellow oil (7.9, g).
Sources & evidence
- ORD record
- ord-adc7a539be124302ad6ccb4ef409ab6e
- Source dataset
- uspto-grants-2006_11
- Patent number
- US07138533B2
Reaction notes
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