5-Chlorovaleryl chloride → HCID 21887238, compound

HRID 722957Notes

Reaction equation

HRID 722957 reaction equation
[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][CH:2]1[NH:10][C:11](=[O:13])[CH3:12].[Cl:14][CH2:15][CH2:16][CH2:17][CH2:18][C:19](Cl)=[O:20]>>[Cl:14][CH2:15][CH2:16][CH2:17][CH2:18][C:19]([C:6]1[CH:5]=[C:4]2[C:9](=[CH:8][CH:7]=1)[CH2:1][CH:2]([NH:10][C:11](=[O:13])[CH3:12])[CH2:3]2)=[O:20]

Participants

3

Procedure

Using N-(2,3-dihydro-1H-inden-2-yl)acetamide and 5-chlorovaleryl chloride according to the same method as that of Reference Example 1, the title compound was obtained as colorless crystals having a melting, point of 106 to 108° C.

Sources & evidence

ORD record
ord-338ccb05f1be44b3864bdd8ebf26c4d3
Source dataset
uspto-grants-2006_11
Patent number
US07138533B2

Reaction notes

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